Xinjiang Agricultural Sciences ›› 2024, Vol. 61 ›› Issue (4): 892-899.DOI: 10.6048/j.issn.1001-4330.2024.04.013
• Agricultural Product Analysis and Detection·Soil Fertilizer·Agricultural Product Processing Engineering • Previous Articles Next Articles
MA Ling1,2,3(), SHEN Qi2,3,4, KANG Qi2,3,4, ZHANG Zhongxiang2,3,4, JIA Hongtao1(), WANG Cheng3,5()
Received:
2023-08-07
Online:
2024-04-20
Published:
2024-05-31
Correspondence author:
JIA Hongtao, WANG Cheng
Supported by:
马凌1,2,3(), 沈琦2,3,4, 康琪2,3,4, 张忠祥2,3,4, 贾宏涛1(), 王成3,5()
通讯作者:
贾宏涛,王成
作者简介:
马凌(1993-),男,四川人,硕士研究生,研究方向为土壤学,(E-mail)519878568@qq.com
基金资助:
CLC Number:
MA Ling, SHEN Qi, KANG Qi, ZHANG Zhongxiang, JIA Hongtao, WANG Cheng. Change and association analysis of five heavy metals in melon plants at different growth stages[J]. Xinjiang Agricultural Sciences, 2024, 61(4): 892-899.
马凌, 沈琦, 康琪, 张忠祥, 贾宏涛, 王成. 甜瓜不同生长阶段5种重金属在植株中富集分配的变化及关联分析[J]. 新疆农业科学, 2024, 61(4): 892-899.
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项目 Items | 重金属含量 Heavy metal content | ||||
---|---|---|---|---|---|
铬Cr (mg/kg) | 镍Ni (mg/kg) | 铜Cu (mg/kg) | 砷As (mg/kg) | 镉Cd (mg/kg) | |
土壤 Soil | 51.687 | 30.305 | 36.736 | 13.025 | 0.287 |
鸡粪 Chicken dung | 14.123 | 23.450 | 28.819 | 4.047 | 0.254 |
Tab.1 Content of 5 heavy metals in soil and soil manure
项目 Items | 重金属含量 Heavy metal content | ||||
---|---|---|---|---|---|
铬Cr (mg/kg) | 镍Ni (mg/kg) | 铜Cu (mg/kg) | 砷As (mg/kg) | 镉Cd (mg/kg) | |
土壤 Soil | 51.687 | 30.305 | 36.736 | 13.025 | 0.287 |
鸡粪 Chicken dung | 14.123 | 23.450 | 28.819 | 4.047 | 0.254 |
步骤 Steps | 控制温度 Controlled temperature (℃) | 升温时间 Heating-up time (min) | 恒温时间 Constant temperature time(min) |
---|---|---|---|
1 | 120 | 5 | 5 |
2 | 150 | 5 | 10 |
3 | 190 | 5 | 20 |
Tab.2 Sample digestion heating sequence
步骤 Steps | 控制温度 Controlled temperature (℃) | 升温时间 Heating-up time (min) | 恒温时间 Constant temperature time(min) |
---|---|---|---|
1 | 120 | 5 | 5 |
2 | 150 | 5 | 10 |
3 | 190 | 5 | 20 |
参数名称 Parameter name | 参数 Parameter | 参数名称 Parameter name | 参数 Parameter |
---|---|---|---|
射频功率Radio-frequency power | 1 500 W | 雾化器 | 高盐/同心雾化器 |
等离子体气流量Plasma body gas flow rate | 15 L/min | 采样锥/截取锥 | 镍/铂锥 |
载气流量Gas flow | 0.80 L/min | 采样深度 | 8 mm ~ 10 mm |
辅助气流量Auxiliary gas flow | 0.40 L/min | 采集模式 | 跳峰 |
氦气流量Helium flow | 4~ 5 mL/min | 检测方式 | 自动 |
雾化室温度Fog chamber temperature | 2 ℃ | 每峰测定点数 | 1 ~ 3 |
样品提升速率Sample lift rate | 0.3 r/s | 重复次数 | 2 ~ 3 |
Tab.3 Operational reference conditions of inductively coupled plasma mass spectrometer
参数名称 Parameter name | 参数 Parameter | 参数名称 Parameter name | 参数 Parameter |
---|---|---|---|
射频功率Radio-frequency power | 1 500 W | 雾化器 | 高盐/同心雾化器 |
等离子体气流量Plasma body gas flow rate | 15 L/min | 采样锥/截取锥 | 镍/铂锥 |
载气流量Gas flow | 0.80 L/min | 采样深度 | 8 mm ~ 10 mm |
辅助气流量Auxiliary gas flow | 0.40 L/min | 采集模式 | 跳峰 |
氦气流量Helium flow | 4~ 5 mL/min | 检测方式 | 自动 |
雾化室温度Fog chamber temperature | 2 ℃ | 每峰测定点数 | 1 ~ 3 |
样品提升速率Sample lift rate | 0.3 r/s | 重复次数 | 2 ~ 3 |
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